[Reu_journal] June 25
Patrick Roberts
roberts_patrick at sbcglobal.net
Mon Jun 25 23:26:43 CDT 2007
June 25, Day 11
My oil did not crystallize so I had to roto-vap the solvent off which gave me my original product back. I then left the oil under high-pressure from a vacuum to evaporate the rest of the solvent off. After the seminar this afternoon, I used the 400 MHz NMR to confirm that I synthesized the correct molecule.
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