[Reu_journal] July 16

Patrick Roberts roberts_patrick at sbcglobal.net
Tue Jul 17 09:36:08 CDT 2007


July 16
  I ran the rest of the acetone off of my column and then ran methanol through it hoping to strip off any product that didn't come off earlier.  I roto-vaped the acetone layer and recovered some product.  I then ran a TLC plate and found the product to show only one spot.  Next I ran an NMR on the product collected from the acetone.  To finish the day, I evaporated the methanol that came through the column, but found no product.
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